Six gas samples were collected from the possum belly (PB) of the shaker assembly during the drilling of NDI Carrara 1. The sample depths ranged from 1187 m to 1360 m and were from organic-rich Proterozoic rock units. The molecular composition and carbon and hydrogen isotope compositions of the individual PB gas components (methane, ethane, propane and carbon dioxide) suggest that the gases were sourced from local, thermally mature, organic-rich shales and siltstones. After taking into account the air and excess nitrogen content in the PB gases, the helium content of the PB gases is low while the molecular hydrogen contents is up to over a 100 times higher than the helium content. Both molecular hydrogen and helium likely have a major radiogenic origin. Based on the results, there is potential for a yet-to-be quantified unconventional hydrocarbon resource in the vicinity of the NDI Carrara 1 well.

The Proterozoic succession in the NDI Carrara 1 drill hole, Northern Territory, consists predominantly of tight shales, siltstones, and calcareous clastic rocks. As part of Geoscience Australia’s Exploring for the Future program, this study aims to derive porosity, permeability and gas content from both laboratory testing and well log interpretation from machine learning approaches, to improve the Proterozoic shale gas reservoir characterisation. The Proterozoic Lawn Hill Formation was divided into four chemostratigraphic packages. The middle two packages were further divided into seven internal units according to principal component analysis and self-organising map clustering on well logs and inorganic geochemical properties. Artificial neural networks were then applied to interpret the mineral compositions, porosity and permeability from well logs, density and neutron-density crossplot interpretations. Gas content was estimated from the interpreted porosity, gas saturation, total organic carbon and clay contents. Petrophysical interpretation results are summarised for all chemostratigraphic packages and units. Package 2 (1116–1430.1 m) has the highest potential among the four chemostratigraphic packages. P2U1 (1116–1271 m) and P2U3 (1335.5–1430.1 m) units have the most favourable petrophysical properties for organic-rich shales with the average total gas contents of 1.25 cm3/g and 1.30 cm3/g, geometric mean permeability of 4.79 µD and 17.56 µD, and net shale thickness of 54.4 m and 85.3 m, respectively. P3U4 unit (687.9–697.9 m) has high gas content and permeability, with the net shale thickness of 29.1 m. Besides the organic-rich shales, the tight non-organic-rich siltstone and shale reservoirs in package 1 (below 1430.1 m) have average gas saturation of 14% and geometric mean permeability of 1.31 µD, respectively. Published in The APPEA Journal 2023. <b>Citation:</b> Wang Liuqi, Bailey Adam H. E., Grosjean Emmanuelle, Carson Chris, Carr Lidena K., Butcher Grace, Boreham Christopher J., Dewhurst Dave, Esteban Lionel, Southby Chris, Henson Paul A. (2023) Petrophysical interpretation and reservoir characterisation on Proterozoic shales in National Drilling Initiative Carrara 1, Northern Territory. <i>The APPEA Journal</i><b> 63</b>, 230-246. https://doi.org/10.1071/AJ22049

<div>NDI Carrara 1 is a deep stratigraphic borehole that was drilled in 2020 under the MinEx CRC’s National Drilling Initiative (NDI) program in collaboration with Geoscience Australia and the Northern Territory Geological Survey. NDI Carrara 1 is the first stratigraphic test of the recently described Carrara Sub-basin, a Proterozoic aged depocentre located in the South Nicholson region of northwest Queensland and the Northern Territory. The borehole was drilled to a total depth of 1751 m and penetrated a succession of Cambrian aged Georgina Basin carbonate and siliciclastic rocks that unconformably overly a thick succession of Proterozoic age siliciclastic and carbonate-rich sediments. Although drilled on the western flank of the Carrara Sub-basin, NDI Carrara 1 did not penetrate to basement. Interpretation of the L210 deep-crustal seismic survey suggests that further Proterozoic sedimentary packages known from the northern Lawn Hill Platform in northwest Queensland are likely to be found underlying the succession intersected in NDI Carrara 1. The borehole was continuously cored from 283 m to total depth, and an extensive suite of wireline logs was acquired. Geoscience Australia and partners have undertaken an extensive analytical program to understand the depositional, structural, and diagenetic history of the sediments intersected in NDI Carrara 1. This program includes a targeted geomechanical study that aims to characterise the physical properties of these Proterozoic rocks through laboratory analysis of core samples, the results of which are summarised in this data release.</div><div><br></div><div>This data release provides data from new unconfined compressive strength (UCS), single-stage triaxial testing, and laboratory ultrasonic testing for 36 sample plugs from NDI Carrara 1. These tests were performed at the CSIRO Geomechanics and Geophysics Laboratory in Perth, during January to June 2022. The full results as provided by CSIRO to Geoscience Australia are provided as an attachment to this document.&nbsp;</div>

<div>NDI Carrara 1 is a deep stratigraphic drill hole completed in 2020 as part of the MinEx CRC National Drilling Initiative (NDI) in collaboration with Geoscience Australia and the Northern Territory Geological Survey. It is the first stratigraphic test of the Carrara Sub-basin, a depocentre newly discovered in the South Nicholson region based on interpretation from seismic surveys (L210 in 2017 and L212 in 2019) acquired as part of the Exploring for the Future program. The drill hole intersected approximately 1120 m of Proterozoic sedimentary rocks unconformably overlain by 630 m of Georgina Basin carbonates.&nbsp;</div><div>Geoscience Australia has undertaken a range of investigations on the lithology, stratigraphy and geotechnical properties of NDI Carrara 1 as well as undertaking a range of analyses of about 500 physical samples recovered through the entire core. Analyses included geochronology, isotope studies, mineralogy, inorganic and organic geochemistry, petrophysics, geomechanics, thermal maturity and petroleum systems investigations.</div><div>Rock-Eval pyrolysis raw data undertaken by Geoscience Australia were reported in Butcher et al. (2021) on selected rock samples to establish their total organic carbon content, hydrocarbon-generating potential and thermal maturity. Interpretation of the Rock-Eval pyrolysis data concluded that a large portion of rocks within the Proterozoic section displayed unreliable Tmax values due to poorly defined S2 peaks resulting from high thermal maturity and low hydrogen content. In order to obtain more reliable Tmax values, Rock-Eval pyrolysis of selected isolated kerogens, where organic matter is concentrated and mineral matrix effects are removed, were conducted and the resulting data are presented in this report.&nbsp;</div><div><br></div>

NDI Carrara 1 is a deep stratigraphic drill hole completed in 2020 as part of the MinEx CRC National Drilling Initiative (NDI) in collaboration with Geoscience Australia and the Northern Territory Geological Survey. It is the first test of the Carrara Sub-Basin, a depocentre newly discovered in the South Nicholson region based on interpretation from seismic surveys (L210 in 2017 and L212 in 2019) recently acquired as part of the Exploring for the Future program. The drill hole intersected approximately 1120 m of Proterozoic sedimentary rocks unconformably overlain by 630 m of Cambrian Georgina Basin carbonates. Continuous cores recovered from 283 m to a total depth of 1750 m provide samples of the highest quality for a comprehensive geochemical program designed to inform on the energy and mineral prospectivity of the Carrara Sub-basin. Total Organic Carbon (TOC) contents from Rock-Eval pyrolysis of the Cambrian and Proterozoic sections demonstrate the potential for several thick black shales as source rocks and unconventional plays. Evidence for retained hydrocarbons included bituminous oil stains in centimetre-scale vugs within the Cambrian Georgina Basin and several oil bleeds within the Proterozoic section. The latter also contains surface gas with up to 2% methane concentrations measured within carbonaceous mudstones. Geochemical analyses of hydrocarbon shows highlight the occurrence of several petroleum systems operating in this frontier region. The results at NDI Carrara 1 offer the promise of a new exciting resource province in northern Australia.

<div>This study was commissioned by Geoscience Australia (GA) to produce a report on methane adsorption and desorption of select samples from the deep stratigraphic drill hole NDI Carrara 1, located in the Proterozoic Carrara Sub-basin in the Northern Territory. Plugs were taken from depths of interest and analysed via adsorption and desorption isotherm testing at the CSIRO laboratories in Clayton, Victoria. </div>

NDI Carrara 1 is a deep stratigraphic drill hole (~1751m) completed in 2020 as part of the MinEx CRC National Drilling Initiative (NDI) in collaboration with Geoscience Australia and the Northern Territory Geological Survey. It is the first test of the Carrara Sub-basin, a depocentre newly discovered in the South Nicholson region based on interpretation from seismic surveys (L210 in 2017 and L212 in 2019) recently acquired as part of the Exploring for the Future program. The drill hole intersected approximately 1100 m of Proterozoic sedimentary rocks uncomformably overlain by 630 m of Cambrian Georgina Basin carbonates. This report presents SHRIMP U-Pb zircon geochronology on 10 volcaniclastic rocks taken from NDI Carrara 1.

The recently drilled deep stratigraphic drill hole NDI Carrara 1 penetrates the carbonate formations of the Cambrian Georgina Basin as well as the underlying Proterozoic successions of the Carrara Sub-basin. The Proterozoic section consists predominantly of tight shales, siltstones, and calcareous clastic rocks. This study aims to assess the petrophysical properties of the Proterozoic shales using conventional wireline logs. Gamma ray and neutron-density crossplots were used to calculate shale volume fraction, and neutron-density crossplots were applied to compute the total and effective porosity of non-shale rocks. Total organic carbon (TOC) content was interpreted using artificial neural networks, and was used to derive the volume of organic matter was converted from TOC content. Bulk density logs were corrected by removing the kerogen effect in the organic-rich shales. Matrix and kerogen densities were obtained by correlating the reciprocal of grain density with TOC content. Total shale porosity was calculated from kerogen-corrected density porosity and organic porosity. Effective porosity was estimated by removing the shaliness effect. Water saturation was derived using the Simandoux equation. The Proterozoic Lawn Hill Formation in NDI Carrara 1 exhibits petrophysical properties that indicate a favourable potential for shale gas resources. Herein, we define three informal intervals within the intersected Lawn Hill Formation; the upper Lawn Hill, the Lawn Hill shale, and the lower Lawn Hill. The net shale thickness of the upper Lawn Hill and Lawn Hill shale intervals are 165 m and 149 m, respectively. The increased TOC content and organic porosity of the upper Lawn Hill and Lawn Hill shale implies higher adsorbed gas content potential. The Lawn Hill shale has the highest gas saturation (average of 31.1%) and the highest potential for free gas content, corresponding to the highest methane responses in logged mud gas profiles. This extended Abstract was submitted to/presented at the Australasian Exploration Geoscience Conference (AEGC) 2023, Brisbane (https://2023.aegc.com.au/)

NDI Carrara 1 is the first stratigraphic test of the Carrara Sub-basin, a newly discovered depocentre in the South Nicholson region that was identified on newly acquired seismic surveys undertaken as part of the Exploring for the Future program. NDI Carrara 1 intersected a thick sequence of Proterozoic aged siliciclastic and carbonate rocks, which host several intervals of interest to hydrocarbon explorers due to affinities with the known Proterozoic shale gas plays of the Beetaloo Sub-basin and the Lawn Hill Platform. These include two organic-rich black shale sequences and a thick sequence of interbedded black shales and silty-sandstones where numerous hydrocarbon shows are demonstrated. An extensive suite of wireline logs was acquired from total depth to the near surface, and continuous core was recovered through the Proterozoic interval. Geoscience Australia and partners are undertaking an extensive program of analytical work to understand the depositional, structural, and diagenetic history of the sediments intersected by NDI Carrara 1, alongside their resource potential. This study characterises petrophysical and geomechanical properties of the Proterozoic interval of NDI Carrara 1 through interpretation of wireline logging data and integration of some of this interpretation with results of geochemical analyses. High interpreted TOC content and a high calculated net shale ratio, alongside high estimated hydrocarbon saturations suggest a high potential for unconventional gas resources in the Proterozoic shale intervals of the Carrara Sub-basin; an assessment supported by gas peaks, particularly methane, measured in mud-logging gas profiles during drilling. Shale brittleness indices and interpreted present-day stresses highlight areas that are likely to be favourable for unconventional gas techniques and which may form attractive shale gas plays. Interpretation of the L210 and L212 seismic surveys suggests that the intersected sequences are laterally extensive and continuous throughout the Carrara Sub-basin, potentially forming a significant new hydrocarbon province and continuing the Proterozoic shale play fairway across the Northern Territory and northwest Queensland. This Abstract was submitted/presented to the 2022 Central Australian Basins Symposium IV (CABS) 29-30 August (https://agentur.eventsair.com/cabsiv/)

<div>NDI Carrara&nbsp;1 is a 1751 m stratigraphic drill hole completed in 2020 as part of the MinEx CRC National Drilling Initiative (NDI). This campaign was a collaboration between Geoscience Australia under the Exploring for the Future program, together with MinEx CRC and the Northern Territory Geological Survey. It is the first drillhole to intersect Proterozoic rocks of the Carrara Sub-basin, a recently discovered depocentre in the South Nicholson region. The drill hole intersected ~625 m of the Paleozoic Georgina Basin, which overlies ~1120 m of Proterozoic carbonates, black shales and siliciclastic rocks, with hydrocarbon shows encountered in both the Paleozoic and Proterozoic sections. Following the completion of the drillhole, a comprehensive analytical program was carried out by Geoscience Australia to better understand the geology of the Carrara Sub-basin and its resource potential.</div><div><br></div><div>Here we present new high-resolution strontium (87Sr/86Sr), carbon (δ13C) and oxygen (δ18O) isotope data from carbonate bearing samples of the Paleozoic Georgina Basin and the Proterozoic Lawn Hill Formation intersected in NDI Carrara&nbsp;1. The aim of this data acquisition was to provide an improved understanding of the paleo-depositional environments and local/global chemostratigraphy trends recorded in the Carrara Sub-basin. </div><div><br></div><div>The majority of samples show significant alteration and thus caution should be exercised when using this data for assessing primary depositional conditions and contemporary sea-water chemistry. Despite the altered nature of most samples, samples belonging to undifferentiated Georgina Basin preserve 87Sr/86Sr ratios close to that of mid-Cambrian seawater, indicating the sampled intervals of Georgina Basin were likely connected to the global Cambrian ocean.&nbsp;Two small positive δ13C excursions (with positive shift in δ18O) within Georgina Basin samples may coincide with reported mid-Cambrian positive δ13C global marine excursions. </div><div><br></div><div>The least altered samples from the Proterozoic Lawn Hill Formation show more radiogenic 87Sr/86Sr values than the expected value of coeval mid-Proterozoic ocean at ~1600 Ma. These radiogenic 87Sr/86Sr values may reflect (i) influx of terrigenous material into a restricted basin with reduced interaction with the global ocean, or (ii) secondary overprinting by more radiogenic diagenetic fluids.</div> Abstract/Poster submitted and presented at 2023 Australian Earth Science Convention (AESC), Perth WA (https://2023.aegc.com.au/)